E-ISSN 2229-7723 | ISSN 0976-9234
 

Original Article 


Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion

Salam M. Nasser, Ahmeed A. Alkarimi, Dakhil N. Taha.

Abstract
Ion exchange chromatography was created using a polymer-based monolithic column as a strong cation-exchange column with various function groups. Acrylic acid (A. acid), glycidyl methacrylate (GMA), and acryl amid were used to make monolithic columns via free radical polymerization (A. amid). The epoxy rings were then sulfonated at 70°C using Na2SO3. A model of common cation of Ni(II) spectrophotometry was used to assess the monolithic column, which was compared to atomic absorption approach. The LOD and LOQ were 0.001 g/mL and 0.002 g/mL, respectively, while the linearity (R2) was 0.9980. FTIR, Brunauer-Emmett-Teller (BET) analysis, and scanning electron microscopy were used to analyze the cation-exchange columns (SEM).

Key words: GMA, Monolith, Ion exchange column, Nickel (II)


 
ARTICLE TOOLS
Abstract
PDF Fulltext
How to cite this articleHow to cite this article
Citation Tools
Related Records
 Articles by Salam M. Nasser
Articles by Ahmeed A. Alkarimi
Articles by Dakhil N. Taha
on Google
on Google Scholar


How to Cite this Article
Pubmed Style

SMN, AAA, Taha DN. Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. PNR. 2022; 13(2): 92-96. doi:10.47750/pnr.2022.13.02.014


Web Style

SMN, AAA, Taha DN. Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. https://www.pnrjournal.com/?mno=55940 [Access: August 11, 2022]. doi:10.47750/pnr.2022.13.02.014


AMA (American Medical Association) Style

SMN, AAA, Taha DN. Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. PNR. 2022; 13(2): 92-96. doi:10.47750/pnr.2022.13.02.014



Vancouver/ICMJE Style

SMN, AAA, Taha DN. Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. PNR. (2022), [cited August 11, 2022]; 13(2): 92-96. doi:10.47750/pnr.2022.13.02.014



Harvard Style

, S. M. N., , A. A. A. & Taha, . D. N. (2022) Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. PNR, 13 (2), 92-96. doi:10.47750/pnr.2022.13.02.014



Turabian Style

, Salam M. Nasser, Ahmeed A. Alkarimi, and Dakhil N. Taha. 2022. Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. Journal of Pharmaceutical Negative Results, 13 (2), 92-96. doi:10.47750/pnr.2022.13.02.014



Chicago Style

, Salam M. Nasser, Ahmeed A. Alkarimi, and Dakhil N. Taha. "Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion." Journal of Pharmaceutical Negative Results 13 (2022), 92-96. doi:10.47750/pnr.2022.13.02.014



MLA (The Modern Language Association) Style

, Salam M. Nasser, Ahmeed A. Alkarimi, and Dakhil N. Taha. "Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion." Journal of Pharmaceutical Negative Results 13.2 (2022), 92-96. Print. doi:10.47750/pnr.2022.13.02.014



APA (American Psychological Association) Style

, S. M. N., , A. A. A. & Taha, . D. N. (2022) Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. Journal of Pharmaceutical Negative Results, 13 (2), 92-96. doi:10.47750/pnr.2022.13.02.014