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2022, Vol: 13, Issue: 1
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Case Report 


Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass

Misde Yola, Mica Tri Kumala Swandari.

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    • Abstract
    ABSTRACT
    Misde Yola *, Patimah *,Mica Tri Kumala Swandari**
    *Lecturer at Department of Pharmacy and Food Analysis, Health Polytechnic of the Ministry of Health, Jakarta II
    ** Lecturer at Department of Pharmacy, Al-Islami College of Health Sciences Al-Itihad, Cilacap, Central Java
    email: misdeyola@gmail.com

    Purpose to determine carbamate , organophosphate, triazole, neonicotinoid pesticide residues in fresh vegetables are still safe for human consumption with Methods Analysis of carbamate residues such as carbofuran and malathion such as organophosphate and prefenofos, imidaclopid, difeconazole , acephate suc a single pesticide in fresh vegetables mustard, cucumber and cabbage. Vegetables come from traditional markets in the Bogor area. Before being analyzed the three vegetables were washed with mineral water, warm water at 60ºC, kitchen salt water and vegetables before washing. The vegetables were homogeneous with a homo mixer blender at 800rpm and after that extracted with acetonitrile with vortex quenchers extraction kit (EN method) for 5 minutes, centrifuge for 5 minutes at 6000rpm speed, supernatant filter with PTFE 13mmx0.22, then input 1 ml supernatant vortex for 5 minutes, centrifuge for 5 minutes at 6000rpm speed, supernatant filter with PTFE 13mmx0.22, then input 1 ml supernatant filtered into LC vials, injection with LCMSMS. Result none of the vegetables analyzed were positive for carbofuran and prefenofos. Conclusion: Consumption of fresh vegetables weighing 20 g / day is still safe for consumption
    Keywords: LC-MS / MS., Carbamate., organophosphate, a single pesticide

    Key words: Keywords: LC-MS / MS., Carbamate., organophosphate, a single pesticide


    		 
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    Pubmed Style

    Yola M, Swandari MTK. Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. PNR. 2021; 12(1): 60-69. doi:10.47750/pnr.2021.12.01.010

    Web Style

    Yola M, Swandari MTK. Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. https://www.pnrjournal.com/?mno=11004 [Access: May 21, 2022]. doi:10.47750/pnr.2021.12.01.010

    AMA (American Medical Association) Style

    Yola M, Swandari MTK. Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. PNR. 2021; 12(1): 60-69. doi:10.47750/pnr.2021.12.01.010


    Vancouver/ICMJE Style

    Yola M, Swandari MTK. Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. PNR. (2021), [cited May 21, 2022]; 12(1): 60-69. doi:10.47750/pnr.2021.12.01.010


    Harvard Style

    Yola, M. & Swandari, . M. T. K. (2021) Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. PNR, 12 (1), 60-69. doi:10.47750/pnr.2021.12.01.010


    Turabian Style

    Yola, Misde, and Mica Tri Kumala Swandari. 2021. Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. Journal of Pharmaceutical Negative Results, 12 (1), 60-69. doi:10.47750/pnr.2021.12.01.010


    Chicago Style

    Yola, Misde, and Mica Tri Kumala Swandari. "Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass." Journal of Pharmaceutical Negative Results 12 (2021), 60-69. doi:10.47750/pnr.2021.12.01.010


    MLA (The Modern Language Association) Style

    Yola, Misde, and Mica Tri Kumala Swandari. "Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass." Journal of Pharmaceutical Negative Results 12.1 (2021), 60-69. Print. doi:10.47750/pnr.2021.12.01.010


    APA (American Psychological Association) Style

    Yola, M. & Swandari, . M. T. K. (2021) Consumption Safety Level of Carbamate, Organo Phosphate,Triazole,Neonicotinoid Pesticide Residues in the Fresh Vegetable Circulating in Bogor According to Analysis of Liquid Cromatography Spectrum Mass. Journal of Pharmaceutical Negative Results, 12 (1), 60-69. doi:10.47750/pnr.2021.12.01.010


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